(2-chlorophenyl)(phenylethynyl)sulfane

Base Information

• Chemical Name: (2-chlorophenyl)(phenylethynyl)sulfane
• CAS No.: 1384843-81-5
• Molecular Formula: C₁₄H₉ClS
• Molecular Weight: 244.744
• Mol file: 1384843-81-5.mol

Synonyms:(2-chlorophenyl)(phenylethynyl)sulfane

Chemical Property of (2-chlorophenyl)(phenylethynyl)sulfane

Chemical Property:

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Technology Process of (2-chlorophenyl)(phenylethynyl)sulfane

There total 1 articles about (2-chlorophenyl)(phenylethynyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

2-chlorothiphenol (6320-03-2) + phenylacetylene (536-74-3) → (2-chlorophenyl)(phenylethynyl)sulfane (1384843-81-5)

Guidance literature:

With oxygen; potassium carbonate; copper(l) chloride; In dimethyl sulfoxide; at 70 ℃; under 760.051 Torr; Schlenk technique;

DOI:10.1021/acs.orglett.1c00273

Reference yield: 78.0%

(2-chlorophenyl)(phenylethynyl)sulfane (1384843-81-5) + benzohydroximoyl chloride (698-16-8) → 4-((2-chlorophenyl)thio)-3,5-diphenylisoxazole

Guidance literature:

With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; triethylamine; In acetonitrile; at 20 ℃; for 13h; Glovebox; Sealed tube;

DOI:10.1021/acs.orglett.1c00273

upstream raw materials:

2-chlorothiphenol

phenylacetylene