(-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one

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Chemical Name:(-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one
CAS No.:1033126-35-0
Molecular Formula:C₃₉H₅₂O₆Si
Molecular Weight:644.924
Hs Code.:

Synonyms:(-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one

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Chemical Property of (-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one

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Technology Process of (-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one

There total 1 articles about (-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1033126-34-9
C₃₉H₅₄O₆Si

: 1033126-35-0
(-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one

Guidance literature:: With dipyridinium dichromate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/jo8004233

Reference yield: 70.0%

: 1033126-35-0
(-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one

: 1822-00-0
trimethylsilylmethyllithium

: 1033126-74-7
C₄₀H₅₄O₅Si

Guidance literature:: (-)-1-((1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutyl)-3,3-dimethylhex-5-en-1-one; trimethylsilylmethyllithium; In tetrahydrofuran; pentane; at 20 ℃; for 1h;

With toluene-4-sulfonic acid; In benzene; at 20 ℃; for 6h; Further stages.;
DOI:10.1021/jo8004233