C₃₁H₃₂BrNO₄

Base Information

Chemical Name:C₃₁H₃₂BrNO₄
CAS No.:1579951-51-1
Molecular Formula:C₃₁H₃₂BrNO₄
Molecular Weight:562.503
Hs Code.:

C<sub>31</sub>H<sub>32</sub>BrNO<sub>4</sub>

Synonyms:C₃₁H₃₂BrNO₄

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Chemical Property of C₃₁H₃₂BrNO₄

Chemical Property:

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Technology Process of C₃₁H₃₂BrNO₄

There total 5 articles about C₃₁H₃₂BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 19614-12-1
2-bromo-5-methoxybenzyl bromide

: C₂₃H₂₅NO₃

: 1579951-51-1
C₃₁H₃₂BrNO₄

Guidance literature:: With lithium hexamethyldisilazane; at -70 - -20 ℃; Inert atmosphere;
DOI:10.1021/op5000489

Reference yield:

: 3128-06-1
5-ketohexanoic acid

: 1579951-51-1
C₃₁H₃₂BrNO₄

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 3 h / 110 °C / Dean-Stark; Inert atmosphere; Large scale

2: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.75 h / -60 - -45 °C / Inert atmosphere; Large scale

3: lithium hexamethyldisilazane / -70 - -20 °C / Inert atmosphere

With toluene-4-sulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;
DOI:10.1021/op5000489

Reference yield:

: 122-99-6,56257-90-0,9004-78-8
2-Phenoxyethanol

: 1579951-51-1
C₃₁H₃₂BrNO₄

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / Inert atmosphere

2: sodium iodide / Inert atmosphere

3: lithium hexamethyldisilazane; 1,4-diaza-bicyclo[2.2.2]octane / methanol; tetrahydrofuran / 10 - 30 °C / Inert atmosphere; Large scale

4: lithium hexamethyldisilazane / -70 - -20 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; triethylamine; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1021/op5000489