2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

Base Information

Chemical Name:2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene
CAS No.:1374751-48-0
Molecular Formula:C₉₀H₈₀B₂O₄
Molecular Weight:1247.24
Hs Code.:

Synonyms:2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

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Chemical Property of 2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

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Technology Process of 2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

There total 1 articles about 2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1374751-47-9
2,5,11,14-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

: 73183-34-3
bis(pinacol)diborane

: 1374751-48-0
2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine; In tert-butyl methyl ether; 1,3,5-trimethyl-benzene; at 80 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol300743f

Reference yield: 76.0%

: 619-42-1
4-methoxycarbonylphenyl bromide

: 1374751-48-0
2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

: C₉₄H₇₀O₄

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In tetrahydrofuran; water; at 60 ℃; for 10h; Inert atmosphere;
DOI:10.1021/jacs.9b07732

Reference yield: 68.0%

: 1374751-48-0
2,11-diboryl-5,8,14,17-tetramesitylhexabenzo[bc,ef,hi,kl,no,qr]coronene

: 1263430-44-9
cis-1,4-bis(4-bromophenyl)-1,4-bis(methoxymethoxy)cyclohexane

: C₁₂₂H₁₀₈Br₂O₈

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; sodium carbonate; In tetrahydrofuran; water; at 66 ℃; for 48h; Inert atmosphere; Darkness;
DOI:10.1039/c6cc03002e