4H-Pyran-4-one,tetrahydro-3,6-dimethyl-2-phenyl-,(2R,3S,6R)-(9CI)

Base Information

Chemical Name:4H-Pyran-4-one,tetrahydro-3,6-dimethyl-2-phenyl-,(2R,3S,6R)-(9CI)
CAS No.:790221-69-1
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:
Mol file:790221-69-1.mol

Synonyms:4H-Pyran-4-one,tetrahydro-3,6-dimethyl-2-phenyl-,(2R,3S,6R)-(9CI)

Suppliers and Price of 4H-Pyran-4-one,tetrahydro-3,6-dimethyl-2-phenyl-,(2R,3S,6R)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4H-Pyran-4-one,tetrahydro-3,6-dimethyl-2-phenyl-,(2R,3S,6R)-(9CI)

Chemical Property:

PSA：26.30000
LogP:2.74170

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4H-Pyran-4-one,tetrahydro-3,6-dimethyl-2-phenyl-,(2R,3S,6R)-(9CI)

There total 4 articles about 4H-Pyran-4-one,tetrahydro-3,6-dimethyl-2-phenyl-,(2R,3S,6R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29478-57-7,29478-58-8,84466-45-5,84466-49-9,99059-93-5
3-hydroxy-3-phenyl-2-methylpropionitrile

: 790221-69-1
syn,syn-3,6-dimethyl-2-phenyl-tetrahydropyran-4-one

: 790221-69-1
anti,anti-3,6-dimethyl-2-phenyl-tetrahydropyran-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride; zinc / tetrahydrofuran / 2 h / 0 - 20 °C

1.2: 0.08 h / 20 °C

2.1: trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran / 18 h / 20 °C

With aluminum (III) chloride; trimethylsilyl trifluoromethanesulfonate; zinc; In tetrahydrofuran; 1.1: Barbier type reaction / 2.1: Michael addition;
DOI:10.1016/j.tet.2012.02.076

Reference yield:

: 29478-57-7,29478-58-8,84466-45-5,84466-49-9,99059-93-5
3-hydroxy-3-phenyl-2-methylpropionitrile

: 790221-69-1
syn,syn-3,6-dimethyl-2-phenyl-tetrahydropyran-4-one

: 790221-69-1
anti,anti-3,6-dimethyl-2-phenyl-tetrahydropyran-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride; zinc / tetrahydrofuran / 2 h / 0 - 20 °C

1.2: 0.08 h / 20 °C

2.1: trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran / 18 h / 20 °C

With aluminum (III) chloride; trimethylsilyl trifluoromethanesulfonate; zinc; In tetrahydrofuran; 1.1: Barbier type reaction / 2.1: Michael addition;
DOI:10.1016/j.tet.2012.02.076