3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester

Base Information

Chemical Name:3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester
CAS No.:193143-31-6
Molecular Formula:C₂₉H₄₆N₂O₈
Molecular Weight:550.693
Hs Code.:

Synonyms:3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester

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Technology Process of 3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester

There total 3 articles about 3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 186349-54-2
di-tert-butyl 2,2'-((2-((2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

: 5437-45-6
Benzyl bromoacetate

: 193143-31-6
3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; water; for 3h; Heating;
DOI:10.1016/j.tetlet.2006.06.128

Reference yield:

: 193143-30-5
di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

: 193143-31-6
3-Benzyloxycarbonylmethyl-6-t-butoxycarbonylmethyl-3,6-diazaoctanedicarboxylic acid-di-t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂ / Pd/C / propan-2-ol / 12 h

2: 90 percent / K₂CO₃ / H₂O; tetrahydrofuran / 3 h / Heating

With hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; water; isopropyl alcohol;
DOI:10.1016/j.tetlet.2006.06.128