di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

Base Information

Chemical Name:di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate
CAS No.:193143-30-5
Molecular Formula:C₂₇H₄₄N₂O₆
Molecular Weight:492.656
Hs Code.:

Synonyms:di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

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Chemical Property of di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

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Technology Process of di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

There total 4 articles about di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 100-39-0
benzyl bromide

: 186349-54-2
di-tert-butyl 2,2'-((2-((2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

: 193143-30-5
di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 35 ℃; for 22h;
DOI:10.1002/ejic.200500018

Reference yield:

: 7662-76-2
tert-butyl 2-(benzylamino)acetate

: 146432-43-1
N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester

: 193143-30-5
di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 10 - 35 ℃; for 24h;

Reference yield:

: 100-52-7
benzaldehyde

: 193143-30-5
di-tert-butyl 2,2'-((2-(benzyl(2-(tert-butoxy)-2-oxoethyl)amino)ethyl)azanediyl)diacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 2 h / cooling

1.2: 80 percent / sodium borohydride / methanol / 7 h / 20 °C

2.1: 83 percent / potassium carbonate / tetrahydrofuran / 3 h / Heating

With potassium carbonate; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2006.06.128