3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate

Base Information

Chemical Name:3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate
CAS No.:1313409-84-5
Molecular Formula:C₁₈H₁₆N₂O₄
Molecular Weight:324.336
Hs Code.:

Synonyms:3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate

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Chemical Property of 3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate

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Technology Process of 3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate

There total 2 articles about 3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13362-30-6
2-amino-4-ethoxycarbonyl-pyridine

: 1313409-83-4
benzyl 2-chloro-3-oxopropanoate

: 1313409-84-5
3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate

Guidance literature:: In tert-butyl alcohol; at 75 ℃; for 4h;

Reference yield:

: 140-18-1
Benzyl chloroacetate

: 1313409-84-5
3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / diethyl ether / 0 - 20 °C

1.2: pH 4 / Cooling

2.1: tert-butyl alcohol / 4 h / 75 °C

With potassium tert-butylate; In diethyl ether; tert-butyl alcohol;

Reference yield:

: 1313409-84-5
3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate

: 7-(ethoxycarbonyl)imidazo[1,2-a]pyridine-3-carboxylic acid hydrochloride

Guidance literature:: 3-benzyl 7-ethyl imidazo[1,2-a]pyridine-3,7-dicarboxylate; With hydrogen; palladium 10% on activated carbon; In ethanol; dichloromethane; for 5h; Inert atmosphere;

With hydrogenchloride; In 1,4-dioxane;