10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

Base Information

Chemical Name:10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole
CAS No.:1022956-62-2
Molecular Formula:C₁₈H₁₅ClN₂O₃S
Molecular Weight:374.848
Hs Code.:

Synonyms:10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

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Chemical Property of 10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

Chemical Property:

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Technology Process of 10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

There total 7 articles about 10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1022956-58-6
10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

: 98-09-9
benzenesulfonyl chloride

: 1022956-62-2
10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

Guidance literature:: 10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole; benzenesulfonyl chloride; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

With water; In N,N-dimethyl-formamide;

Reference yield:

: 1022955-54-9
N-(2-{[1-(phenylsulfonyl)-1H-indol-5-yl]oxy}ethyl)acetamide

: 1022956-62-2
10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

Guidance literature:: Multi-step reaction with 4 steps

1: N-chloro-succinimide / tetrahydrofuran / 6 h / 20 - 40 °C

2: sodium hydroxide; water / ethanol / 1 h / 75 °C

3: trichlorophosphate / acetonitrile / 0.25 h / 120 °C / Microwave irradiation

4: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C

With sodium hydroxide; N-chloro-succinimide; water; sodium hydride; trichlorophosphate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: C₂₃H₂₆N₂O₆S

: 1022956-62-2
10-chloro-1-methyl-8-(phenylsulfonyl)-3,8-dihydro-4H-[1,4]oxazepino[6,7-e]indole

Guidance literature:: Multi-step reaction with 6 steps

1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

2: dmap; triethylamine / dichloromethane / 1 h / 0 - 20 °C

3: N-chloro-succinimide / tetrahydrofuran / 6 h / 20 - 40 °C

4: sodium hydroxide; water / ethanol / 1 h / 75 °C

5: trichlorophosphate / acetonitrile / 0.25 h / 120 °C / Microwave irradiation

6: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C

With dmap; sodium hydroxide; N-chloro-succinimide; water; sodium hydride; triethylamine; trifluoroacetic acid; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;