4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside
CAS No.:1261222-55-2
Molecular Formula:C₆₁H₅₄O₁₅S
Molecular Weight:1059.16
Hs Code.:

Synonyms:4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

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Chemical Property of 4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

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Technology Process of 4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

There total 1 articles about 4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1261222-54-1
C₆₁H₅₂O₁₅S

: 1261222-55-2
4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

Guidance literature:: C₆₁H₅₂O₁₅S; With sodium cyanoborohydride; In tetrahydrofuran; for 0.0833333h; Molecular sieve;

With iodine; In tetrahydrofuran; for 2h; regiospecific reaction; Molecular sieve;
DOI:10.1016/j.carres.2010.10.013

Reference yield:

: 1261222-55-2
4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

: 1363157-77-0
p-methylphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-deoxy-1-thio-β-D-glucopyranoside

: C₉₄H₉₆O₂₀SSi

Guidance literature:: p-methylphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-deoxy-1-thio-β-D-glucopyranoside; With silver trifluoromethanesulfonate; In diethyl ether; at -78 ℃; for 0.166667h; Molecular sieve;

With p-methylbenzenesulfenyl chloride; In diethyl ether; at -78 ℃; for 0.25h; Molecular sieve;

4-methylphenyl 2,3,6-tri-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-benzyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside; In diethyl ether; dichloromethane; at -78 - 20 ℃; for 1.5h; stereoselective reaction; Molecular sieve;
DOI:10.1021/acs.orglett.9b00653