4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride

Base Information

Chemical Name:4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride
CAS No.:80874-14-2
Molecular Formula:C₂₃H₃₁N₃O₄S*ClH
Molecular Weight:482.044
Hs Code.:

Synonyms:4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride

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Chemical Property of 4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride

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Technology Process of 4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride

There total 5 articles about 4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 64-17-5
ethanol

: 80852-61-5
N-Butyl-3-(4-cyano-phenyl)-2-(toluene-4-sulfonylamino)-propionamide

: 80874-14-2
4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 0 - 5 ℃;

Reference yield:

: 52117-01-8
N-acetyl-4-cyano-α-(ethoxycarbonyl)phenylalanine ethyl ester

: 80874-14-2
4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

2: SOCl₂ / 1 h / Heating

3: 83 percent / benzene / 1.5 h / Ambient temperature

4: 83 percent / HCl(gas) / dioxane / 0 - 5 °C

With hydrogenchloride; thionyl chloride; In 1,4-dioxane; benzene;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 80874-14-2
4-[2-Butylcarbamoyl-2-(toluene-4-sulfonylamino)-ethyl]-benzimidic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

2: SOCl₂ / 1 h / Heating

3: 83 percent / benzene / 1.5 h / Ambient temperature

4: 83 percent / HCl(gas) / dioxane / 0 - 5 °C

With hydrogenchloride; thionyl chloride; In 1,4-dioxane; benzene;