Technology Process of C23H36O4Si
There total 8 articles about C23H36O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
2.1: di(n-butyl)tin oxide / toluene / 3 h
2.2: 3 h / 20 °C / Molecular sieve
3.1: Dess-Martin periodane / dichloromethane / 3 h / 0 °C
4.1: tributylphosphine / methanol; chloroform; water / 20 °C
5.1: dmap; triethylamine / dichloromethane / 2 h / 20 °C
With
dmap; tributylphosphine; diisobutylaluminium hydride; di(n-butyl)tin oxide; Dess-Martin periodane; triethylamine;
In
methanol; dichloromethane; chloroform; water; toluene;
4.1: Morita-Baylis-Hillman reaction;
DOI:10.1016/j.bmcl.2012.01.006
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride / tetrahydrofuran / 3 h / 20 °C
2.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
3.1: di(n-butyl)tin oxide / toluene / 3 h
3.2: 3 h / 20 °C / Molecular sieve
4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 °C
5.1: tributylphosphine / methanol; chloroform; water / 20 °C
6.1: dmap; triethylamine / dichloromethane / 2 h / 20 °C
With
hydrogenchloride; dmap; tributylphosphine; diisobutylaluminium hydride; di(n-butyl)tin oxide; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; water; toluene;
5.1: Morita-Baylis-Hillman reaction;
DOI:10.1016/j.bmcl.2012.01.006