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C23H36O4Si

Base Information Edit
C<sub>23</sub>H<sub>36</sub>O<sub>4</sub>Si

Synonyms:C23H36O4Si

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C23H36O4Si Edit
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Technology Process of C23H36O4Si

There total 8 articles about C23H36O4Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2012.01.006
Guidance literature:
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
2.1: di(n-butyl)tin oxide / toluene / 3 h
2.2: 3 h / 20 °C / Molecular sieve
3.1: Dess-Martin periodane / dichloromethane / 3 h / 0 °C
4.1: tributylphosphine / methanol; chloroform; water / 20 °C
5.1: dmap; triethylamine / dichloromethane / 2 h / 20 °C
With dmap; tributylphosphine; diisobutylaluminium hydride; di(n-butyl)tin oxide; Dess-Martin periodane; triethylamine; In methanol; dichloromethane; chloroform; water; toluene; 4.1: Morita-Baylis-Hillman reaction;
DOI:10.1016/j.bmcl.2012.01.006
Guidance literature:
Multi-step reaction with 6 steps
1.1: hydrogenchloride / tetrahydrofuran / 3 h / 20 °C
2.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
3.1: di(n-butyl)tin oxide / toluene / 3 h
3.2: 3 h / 20 °C / Molecular sieve
4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 °C
5.1: tributylphosphine / methanol; chloroform; water / 20 °C
6.1: dmap; triethylamine / dichloromethane / 2 h / 20 °C
With hydrogenchloride; dmap; tributylphosphine; diisobutylaluminium hydride; di(n-butyl)tin oxide; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; toluene; 5.1: Morita-Baylis-Hillman reaction;
DOI:10.1016/j.bmcl.2012.01.006
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