2-S-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-2-thiopseudourea hydrobromide

Base Information Edit

Chemical Name:2-S-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-2-thiopseudourea hydrobromide
CAS No.:57030-42-9
Molecular Formula:BrH*C₁₅H₂₂N₂O₉S
Molecular Weight:487.326
Hs Code.:
Mol file:57030-42-9.mol

Synonyms:2-S-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-2-thiopseudourea hydrobromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-S-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-2-thiopseudourea hydrobromide Edit

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Technology Process of 2-S-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-2-thiopseudourea hydrobromide

There total 11 articles about 2-S-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-2-thiopseudourea hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 17356-08-0
thiourea

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 40591-65-9,51224-13-6,51898-28-3,57030-42-9,106818-92-2
2,3,4,6-tetra-O-acetylgalactopyranosyl-1-β-pseudothiourea hydrobromide

Guidance literature:: In acetone; for 0.05h; microwave irradiation;
DOI:10.1080/07328300500282540

Reference yield: 76.0%

: 10257-28-0
D-Galactose

: 108-24-7
acetic anhydride

: 17356-08-0
thiourea

: 40591-65-9,51224-13-6,51898-28-3,57030-42-9,106818-92-2
2,3,4,6-tetra-O-acetylgalactopyranosyl-1-β-pseudothiourea hydrobromide

Guidance literature:: D-Galactose; acetic anhydride; With perchloric acid; at 20 - 25 ℃; for 1.5h;

With hydrogen bromide; at 15 ℃; for 1h;

thiourea; In acetonitrile; at 60 - 70 ℃; for 0.5h;