[2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione

Base Information

• Chemical Name: [2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione
• CAS No.: 121150-38-7
• Molecular Formula: C₁₇H₁₅ClO₂S
• Molecular Weight: 318.824
• Mol file: 121150-38-7.mol

Synonyms:[2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione

Chemical Property of [2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione

There total 2 articles about [2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

[2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanone (121150-33-2) → [2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione (121150-38-7)

Guidance literature:

With tetraphosphorus decasulfide; In tetrahydrofuran; Heating;

DOI:10.1016/S0040-4039(00)95156-6

Reference yield:

Benzophenone-3 (131-57-7,897050-18-9) → [2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione (121150-38-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / K₂CO₃

2: 82 percent / P₄S₁₀ / tetrahydrofuran / Heating

With tetraphosphorus decasulfide; potassium carbonate; In tetrahydrofuran;

DOI:10.1016/S0040-4039(00)95156-6

Reference yield: 78.0%

[2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanethione (121150-38-7) → (E)-3-Chloro-9-methoxy-6-phenyl-4H,6H-benzo[b][1,5]oxathiocine (134617-20-2)

Guidance literature:

In xylene; for 24h; Heating;

DOI:10.1016/S0040-4039(00)95156-6

upstream raw materials:

[2-(2-Chloro-allyloxy)-4-methoxy-phenyl]-phenyl-methanone

Benzophenone-3

Downstream raw materials:

(E)-3-Chloro-9-methoxy-6-phenyl-4H,6H-benzo[b][1,5]oxathiocine

3a-Chloro-7-methoxy-9b-phenyl-3a,9b-dihydro-3H,4H-[1,2]dithiolo[4,3-c]chromene