Technology Process of C24H40O6Si
There total 12 articles about C24H40O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: boron trifluoride diethyl etherate / diethyl ether / 0 °C
2.1: sodium periodate; ruthenium trichloride; water; zinc(II) chloride / ethyl acetate; acetonitrile / 0 °C
3.1: toluene-4-sulfonic acid / tetrahydrofuran / 40 °C
4.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C
5.1: sodium hydride / tetrahydrofuran / 0 °C
5.2: 0 - 20 °C
6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C
With
ruthenium trichloride; sodium tetrahydroborate; sodium periodate; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; water; tri-n-butyl-tin hydride; sodium hydride; toluene-4-sulfonic acid; zinc(II) chloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile; benzene;
6.1: Barton-McCombie deoxygenation;
DOI:10.1016/j.tetlet.2012.06.005
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium periodate; ruthenium trichloride; water; zinc(II) chloride / ethyl acetate; acetonitrile / 0 °C
2.1: toluene-4-sulfonic acid / tetrahydrofuran / 40 °C
3.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C
4.1: sodium hydride / tetrahydrofuran / 0 °C
4.2: 0 - 20 °C
5.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C
With
ruthenium trichloride; sodium tetrahydroborate; sodium periodate; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; sodium hydride; toluene-4-sulfonic acid; zinc(II) chloride;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetonitrile; benzene;
5.1: Barton-McCombie deoxygenation;
DOI:10.1016/j.tetlet.2012.06.005