4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Base Information

Chemical Name:4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester
CAS No.:1437306-82-5
Molecular Formula:C₂₄H₃₉NO₁₀
Molecular Weight:501.574
Hs Code.:

Synonyms:4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

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Chemical Property of 4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

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Technology Process of 4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

There total 4 articles about 4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1437306-81-4
4-(2-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

: 1437306-82-5
4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Guidance literature:: In methanol; tert-butyl alcohol; at 20 ℃;
DOI:10.1021/bc400074w

Reference yield:

: 3943-80-4
4-hydroxy-3,5-dimethoxybenzoic acid ethyl ester

: 1437306-82-5
4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 70 °C

2: palladium diacetate; hydrogen / ethanol

3: methanol; tert-butyl alcohol / 20 °C

With hydrogen; palladium diacetate; caesium carbonate; In methanol; ethanol; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/bc400074w

Reference yield:

: 530-57-4
3,5-dimethoxy-4-hydroxybenzoic acid

: 1437306-82-5
4-(2-(2-(2-(2-N-Boc-aminoethoxy)ethoxy)ethoxy)ethoxy)-3,5-dimethoxybenzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 0 - 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 4 h / 70 °C

3: palladium diacetate; hydrogen / ethanol

4: methanol; tert-butyl alcohol / 20 °C

With thionyl chloride; hydrogen; palladium diacetate; caesium carbonate; In methanol; ethanol; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/bc400074w