3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester

Base Information

• Chemical Name: 3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester
• CAS No.: 66889-29-0
• Molecular Formula: C₁₈H₁₉N₃O₆S₂
• Molecular Weight: 437.497

Synonyms:3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester

Chemical Property of 3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester

Chemical Property:

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Technology Process of 3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester

There total 2 articles about 3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium-p-thiocresolate (918667-29-5) + 3-nitro-4-chloro-5-N,N-dimethylaminomethyleneaminosulphonyl-benzoic acid methyl ester (60376-77-4) → 3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester (66889-29-0)

Guidance literature:

In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl-formamide;

Reference yield:

→ 3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester (66889-29-0)

Guidance literature:

Thiokresol, entspr. Chlorid;

Reference yield:

3-nitro-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester (66889-29-0) → 3-amino-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester (66889-30-3)

Guidance literature:

With hydrogen; aluminum nickel; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl-formamide;

upstream raw materials:

potassium-p-thiocresolate

3-nitro-4-chloro-5-N,N-dimethylaminomethyleneaminosulphonyl-benzoic acid methyl ester

Downstream raw materials:

3-amino-4-(4'-methylphenylthio)-5-N,N-dimethylaminomethylene-aminosulfonyl benzoic acid methyl ester

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