2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol

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Chemical Name:2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol
CAS No.:380414-43-7
Molecular Formula:C₃₉H₅₆O₅Si₂
Molecular Weight:661.042
Hs Code.:

Synonyms:2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol

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Chemical Property of 2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol

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Technology Process of 2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol

There total 3 articles about 2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 380414-40-4
1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

: 380414-43-7
2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol

Guidance literature:: With 1H-imidazole; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(98)80045-2

Reference yield:

: 380414-39-1
2-[(S)-5-Methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-5H-furan-(2Z)-ylidene]-ethanol

: 380414-43-7
2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyldioxirane / acetone / 0 °C

2: 80 percent / imidazole / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; 3,3-dimethyldioxirane; In dichloromethane; acetone;
DOI:10.1016/S0040-4039(98)80045-2

Reference yield:

: 380414-38-0
[(S)-5-Methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-5H-furan-(2Z)-ylidene]-acetic acid ethyl ester

: 380414-43-7
2-(tert-Butyl-diphenyl-silanyloxy)-1-[(S)-2-methoxy-5-methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-2,5-dihydro-furan-2-yl]-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminum hydride / diethyl ether / 0 °C

2: dimethyldioxirane / acetone / 0 °C

3: 80 percent / imidazole / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; 3,3-dimethyldioxirane; In diethyl ether; dichloromethane; acetone;
DOI:10.1016/S0040-4039(98)80045-2