1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

Base Information

Chemical Name:1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol
CAS No.:380414-40-4
Molecular Formula:C₂₃H₃₈O₅Si
Molecular Weight:422.637
Hs Code.:

Synonyms:1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

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Chemical Property of 1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

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Technology Process of 1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

There total 5 articles about 1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 74087-85-7
3,3-dimethyldioxirane

: 380414-39-1
2-[(S)-5-Methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-5H-furan-(2Z)-ylidene]-ethanol

: 380414-40-4
1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

Guidance literature:: In methanol; acetone; at 0 ℃; for 0.0833333h;
DOI:10.1016/S0040-4020(01)00739-6

Reference yield:

: 67-56-1
methanol

: 380414-39-1
2-[(S)-5-Methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-5H-furan-(2Z)-ylidene]-ethanol

: 380414-40-4
1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

Guidance literature:: With 3,3-dimethyldioxirane; In acetone; at 0 ℃; Yield given;
DOI:10.1016/S0040-4039(98)80045-2

Reference yield:

: 380414-38-0
[(S)-5-Methyl-5-((S)-3-phenyl-1-triethylsilanyloxy-propyl)-5H-furan-(2Z)-ylidene]-acetic acid ethyl ester

: 380414-40-4
1-[(5S)-2-methoxy-5-methyl-5-(3-phenyl-1S-triethylsilanyloxy-propyl)-2,5-dihydrofuran-2-yl]-ethanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 152 mg / LiAlH₄ / diethyl ether / 1 h / 0 °C

2: 97 percent / methanol; acetone / 0.08 h / 0 °C

With lithium aluminium tetrahydride; In methanol; diethyl ether; acetone;
DOI:10.1016/S0040-4020(01)00739-6