C₃₈H₃₂F₂IN₅O₅

Base Information

Chemical Name:C₃₈H₃₂F₂IN₅O₅
CAS No.:1613589-65-3
Molecular Formula:C₃₈H₃₂F₂IN₅O₅
Molecular Weight:803.604
Hs Code.:

C<sub>38</sub>H<sub>32</sub>F<sub>2</sub>IN<sub>5</sub>O<sub>5</sub>

Synonyms:C₃₈H₃₂F₂IN₅O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₈H₃₂F₂IN₅O₅

Chemical Property:

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Technology Process of C₃₈H₃₂F₂IN₅O₅

There total 12 articles about C₃₈H₃₂F₂IN₅O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1613589-64-2
C₃₁H₂₈F₂IN₅O₄

: 98-88-4
benzoyl chloride

: 1613589-65-3
C₃₈H₃₂F₂IN₅O₅

Guidance literature:: With pyridine; at 0 - 20 ℃; for 3h;

Reference yield:

: 874638-80-9,1033394-94-3
((2R,3R,4R)-3-benzoyloxy-4-fluoro-4-methyl-5-oxo-tetrahydrofuran-2-yl)methyl benzoate

: 1613589-65-3
C₃₈H₃₂F₂IN₅O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 1 h / -78 - -20 °C / Inert atmosphere

2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.33 h / -25 - -20 °C / Inert atmosphere

3.1: potassium tert-butylate / acetonitrile; tert-butyl alcohol / 0.5 h / 35 °C

3.2: 50 °C

4.1: silver nitrate / dichloromethane / 20 °C

4.2: 12 h / 20 °C

5.1: triphenylphosphine; pyridine; iodine / 20 °C

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 4 h / Reflux

7.1: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 20 °C / Cooling with ice

8.1: pyridine / 3 h / 0 - 20 °C

With pyridine; N-iodo-succinimide; carbon tetrabromide; potassium tert-butylate; iodine; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); lithium tri-t-butoxyaluminum hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile; tert-butyl alcohol;

Reference yield:

: 1199809-24-9
(((2R,3R,4R,5R)-3-(benzoyloxy)-5-bromo-4-fluoro-4-methyltetrahydrofuran-2-yl)methyl benzoate)

: 1613589-65-3
C₃₈H₃₂F₂IN₅O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium tert-butylate / acetonitrile; tert-butyl alcohol / 0.5 h / 35 °C

1.2: 50 °C

2.1: silver nitrate / dichloromethane / 20 °C

2.2: 12 h / 20 °C

3.1: triphenylphosphine; pyridine; iodine / 20 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 4 h / Reflux

5.1: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 2 h / 20 °C / Cooling with ice

6.1: pyridine / 3 h / 0 - 20 °C

With pyridine; N-iodo-succinimide; potassium tert-butylate; iodine; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile; tert-butyl alcohol;