4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline

Base Information

Chemical Name:4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline
CAS No.:1332526-29-0
Molecular Formula:C₁₈H₁₉N₃O₃S
Molecular Weight:357.433
Hs Code.:

Synonyms:4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline

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Chemical Property of 4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline

Chemical Property:

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Technology Process of 4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline

There total 3 articles about 4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.5%

: 221640-38-6
4-(1H-imidazol-2-yl)-N,N-dimethylaniline

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 1332526-29-0
4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline

Guidance literature:: 4-(1H-imidazol-2-yl)-N,N-dimethylaniline; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.333333h; Inert atmosphere;

4-methoxy-phenyl-sulphonyl chloride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2011.06.084

Reference yield: 61.5%

: 1332526-29-0
4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline

Guidance literature:

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 1332526-29-0
4-(1-((4-methoxyphenyl)sulfonyl)-1H-imidazol-2-yl)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium hydroxide / ethanol; water / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With ammonium hydroxide; sodium hydride; In tetrahydrofuran; ethanol; water; mineral oil;
DOI:10.1016/j.bmc.2011.06.084