Technology Process of 3-phenylpropanoic dithioperoxyanhydride
There total 7 articles about 3-phenylpropanoic dithioperoxyanhydride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium sulfide; tetrabutylammomium bromide;
In
water; toluene;
at 20 ℃;
for 1h;
DOI:10.1021/acs.orglett.6b02818
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / DCC, 4-dimethylaminopyridine / CH2Cl2
2: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature
3: dicyclohexylcarbodiimide / CH2Cl2
4: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2 / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt
With
carbon disulfide; dmap; sodium hydroxide; n-butyllithium; dicyclohexyl-carbodiimide; 1,1,1,3,3,3-hexamethyl-disilazane;
In
ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)85980-9
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 3 N aq. NaOH / ethanol / 12 h / Ambient temperature
2: dicyclohexylcarbodiimide / CH2Cl2
3: 1.) hexamethyldisilazane, 1.6 M n-BuLi, 2.) CS2 / 1.) THF, hexane, -20 deg C, 30 min, 2.) THF, rt
With
carbon disulfide; sodium hydroxide; n-butyllithium; dicyclohexyl-carbodiimide; 1,1,1,3,3,3-hexamethyl-disilazane;
In
ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)85980-9
