2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Base Information

• Chemical Name: 2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester
• CAS No.: 760197-70-4
• Molecular Formula: C₂₆H₃₀O₃
• Molecular Weight: 390.522

Synonyms:2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Chemical Property of 2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

Chemical Property:

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Technology Process of 2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

There total 1 articles about 2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

exo-10,10-diphenyl-10-hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-ol (221099-71-4) + Methacryloyl chloride (920-46-7,26937-45-1) → 2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (760197-70-4)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

DOI:10.1016/j.tetasy.2008.02.028

Reference yield:

N-aminophthalamide (1875-48-5) + 2-methyl-acrylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (760197-70-4) → (2S)-1-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-methylaziridine-2-carboxylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester + (2R)-1-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-methylaziridine-2-carboxylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester (1030379-37-3)

Guidance literature:

With lead(IV) acetate; In tetrahydrofuran; at 0 ℃; for 0.166667h;

DOI:10.1016/j.tetasy.2008.02.028

upstream raw materials:

exo-10,10-diphenyl-10-hydroxymethyl-7,7-dimethylbicyclo[2.2.1]heptane-2-ol

Methacryloyl chloride

Downstream raw materials:

(2R)-1-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-methylaziridine-2-carboxylic acid 1-[hydroxy(diphenyl)methyl]-7,7-dimethyl-bicyclo[2.2.1]hept-2-yl ester

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