C₅₀H₄₆BF₂N₇O₂S

Base Information

• Chemical Name: C₅₀H₄₆BF₂N₇O₂S
• CAS No.: 1290570-26-1
• Molecular Formula: C₅₀H₄₆BF₂N₇O₂S
• Molecular Weight: 857.835
• Mol file: 1290570-26-1.mol

Synonyms:C₅₀H₄₆BF₂N₇O₂S

Chemical Property of C₅₀H₄₆BF₂N₇O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₀H₄₆BF₂N₇O₂S

There total 3 articles about C₅₀H₄₆BF₂N₇O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

C43H39BF2N4O3 (1290570-25-0) + phenyl isothiocyanate (103-72-0) → C50H46BF2N7O2S (1290570-26-1)

Guidance literature:

C₄₃H₃₉BF₂N₄O₃; With hydrazine hydrate; In methanol; at 60 ℃; for 6h;

phenyl isothiocyanate; In N,N-dimethyl-formamide; at 60 ℃; for 4h;

DOI:10.1002/chem.201002498

Reference yield:

5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide (1264756-25-3) → C50H46BF2N7O2S (1290570-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: palladium diacetate; sodium carbonate; triphenylphosphine / methanol; propan-1-ol / 6 h / 75 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol / 6 h / 60 °C

2.2: 4 h / 60 °C

With palladium diacetate; sodium carbonate; hydrazine hydrate; triphenylphosphine; In methanol; propan-1-ol; 1.1: Suzuki coupling;

DOI:10.1002/chem.201002498

Reference yield:

C24H21BrN2O3 (1290102-36-1) → C50H46BF2N7O2S (1290570-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: palladium diacetate; sodium carbonate; triphenylphosphine / methanol; propan-1-ol / 6 h / 75 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol / 6 h / 60 °C

2.2: 4 h / 60 °C

With palladium diacetate; sodium carbonate; hydrazine hydrate; triphenylphosphine; In methanol; propan-1-ol; 1.1: Suzuki coupling;

DOI:10.1002/chem.201002498

upstream raw materials:

5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

C₂₄H₂₁BrN₂O₃

C₄₃H₃₉BF₂N₄O₃

phenyl isothiocyanate