5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Name:5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide
CAS No.:1264756-25-3
Molecular Formula:C₂₅H₃₀B₂F₂N₂O₂
Molecular Weight:450.144
Hs Code.:

Synonyms:5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Property of 5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

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Technology Process of 5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

There total 12 articles about 5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 10-(4-bromophenyl)-5,5-difluoro-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 73183-34-3
bis(pinacol)diborane

: 1264756-25-3
5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In tetrahydrofuran;
DOI:10.1021/ac301456s

Reference yield: 69.0%

: C₁₉H₁₉BBrF₂N₂

: 73183-34-3
bis(pinacol)diborane

: 1264756-25-3
5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In water; toluene; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201001188

Reference yield: 30.0%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 109-63-7
boron trifluoride diethyl etherate

: 128376-64-7
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

: 1264756-25-3
5,5-difluoro-1,3,7,9-tetramethyl-10-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-5H-dipyrrolo[1,2-c:1',2'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: 2,4-dimethyl-1H-pyrrole; 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde; With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h;

boron trifluoride diethyl etherate; With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1142/S108842461850058X