benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside
CAS No.:75263-24-0
Molecular Formula:C₁₉H₂₇NO₈S
Molecular Weight:429.491
Hs Code.:

Synonyms:benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside

There total 1 articles about benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 66026-10-6
N-((4aR,6S,7R,8R,8aS)-6-(benzyloxy)-8-hydroxy-2,2-dimethylhexahydropyrano[3,2-d][1,3]dioxin-7-yl)acetamide

: 124-63-0
methanesulfonyl chloride

: 75263-24-0
benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside

Guidance literature:: With pyridine; at 0 ℃; for 4h;
DOI:10.1016/S0008-6215(00)80713-2

Reference yield: 79.0%

: 75263-24-0
benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside

: 75263-30-8
benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-α-D-allopyranosidede

Guidance literature:: With water; sodium acetate; In 2-methoxy-ethanol; for 38h; Heating;
DOI:10.1016/S0008-6215(00)80713-2

Reference yield:

: 75263-24-0
benzyl 2-acetamido-2-deoxy-4,6-isopropylidene-3-O-mesyl-α-D-glucopyranoside

: benzyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-3-O-(D-2-propanoyl-L-alanyl-D-isoglutamine benzyl ester)-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / sodium acetate, H₂O / 2-methoxy-ethanol / 38 h / Heating

2: 71 percent / sodium hydride / dioxane / 2 h / 65 °C

3: 95 percent / N-hydroxysuccinimide, dicyclohexylcarbodiimide, triethylamine / dioxane / 1 h / Ambient temperature

With 1-hydroxy-pyrrolidine-2,5-dione; water; sodium acetate; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; 2-methoxy-ethanol;
DOI:10.1016/S0008-6215(00)80713-2