(E)-1,2,3-Triphenyl-allylideneamine

Base Information

Chemical Name:(E)-1,2,3-Triphenyl-allylideneamine
CAS No.:261171-22-6
Molecular Formula:C₂₁H₁₇N
Molecular Weight:283.373
Hs Code.:

Synonyms:(E)-1,2,3-Triphenyl-allylideneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1,2,3-Triphenyl-allylideneamine

Chemical Property:

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Technology Process of (E)-1,2,3-Triphenyl-allylideneamine

There total 4 articles about (E)-1,2,3-Triphenyl-allylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 3-azido-1,2,3-triphenyl-1-propene

: 261171-22-6
(E)-1,2,3-Triphenyl-allylideneamine

Guidance literature:: With phosphazene base-P₄-tert-butyl; In hexane; benzene; at 20 ℃; for 1h;

Reference yield:

: 3239-32-5
(Z)-1,2,3-triphenylprop-1-ene

: 261171-22-6
(E)-1,2,3-Triphenyl-allylideneamine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / m-chloroperbenzoic acid; NaHCO₃ / CH₂Cl₂ / 20 °C

2: 61 percent / NaN₃ / dimethylformamide; H₂O / 120 h / 100 °C

3: 31 percent / thionyl chloride; pyridine / 0.5 h / -10 °C

4: 89 percent / [(Me₂N)3P=N]3P=NtBu / benzene; hexane / 1 h / 20 °C

With pyridine; thionyl chloride; sodium azide; sodium hydrogencarbonate; phosphazene base-P₄-tert-butyl; 3-chloro-benzenecarboperoxoic acid; In hexane; dichloromethane; water; N,N-dimethyl-formamide; benzene; 1: Oxidation / 2: Ring cleavage / 3: Dehydration / 4: Elimination;

Reference yield:

: cis-2-benzyl-2,3-diphenyloxirane

: 261171-22-6
(E)-1,2,3-Triphenyl-allylideneamine

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / NaN₃ / dimethylformamide; H₂O / 120 h / 100 °C

2: 31 percent / thionyl chloride; pyridine / 0.5 h / -10 °C

3: 89 percent / [(Me₂N)3P=N]3P=NtBu / benzene; hexane / 1 h / 20 °C

With pyridine; thionyl chloride; sodium azide; phosphazene base-P₄-tert-butyl; In hexane; water; N,N-dimethyl-formamide; benzene; 1: Ring cleavage / 2: Dehydration / 3: Elimination;