Technology Process of C19H29FO5
There total 5 articles about C19H29FO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H29FO6;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1.25h;
Inert atmosphere;
With
water; ammonium chloride;
In
tetrahydrofuran; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; mercury dichloride; zinc / toluene; water / 72 h / Reflux
2.1: potassium hydroxide; potassium nitrososulfonate / water; acetone / 40 h / 20 °C / pH 8
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -78 - -10 °C / Inert atmosphere
3.2: 14.17 h / -78 - 20 °C
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; lithium aluminium tetrahydride; potassium nitrososulfonate; mercury dichloride; potassium hydroxide; zinc; lithium diisopropyl amide;
In
tetrahydrofuran; water; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum (III) chloride / nitrobenzene / 17 h / 0 - 20 °C / Inert atmosphere
1.2: 0.33 h / pH 1 - 2
2.1: hydrogenchloride; mercury dichloride; zinc / toluene; water / 72 h / Reflux
3.1: potassium hydroxide; potassium nitrososulfonate / water; acetone / 40 h / 20 °C / pH 8
4.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -78 - -10 °C / Inert atmosphere
4.2: 14.17 h / -78 - 20 °C
5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; aluminum (III) chloride; lithium aluminium tetrahydride; potassium nitrososulfonate; mercury dichloride; potassium hydroxide; zinc; lithium diisopropyl amide;
In
tetrahydrofuran; water; nitrobenzene; acetone; toluene;