(E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

Base Information

Chemical Name:(E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime
CAS No.:1390649-38-3
Molecular Formula:C₂₉H₂₄N₄O₅
Molecular Weight:508.533
Hs Code.:

Synonyms:(E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

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Chemical Property of (E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

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Technology Process of (E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

There total 4 articles about (E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1390649-36-1
(E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime

: 108-24-7
acetic anhydride

: 1390649-38-3
(E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

Guidance literature:: With pyridine; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2012.05.035

Reference yield:

: 191801-89-5
6-chloro-9-methoxy-11H-indeno[1,2-c]quinolin-11-one

: 1390649-38-3
(E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / 2-ethoxy-ethanol / 1 h / Microwave irradiation

2: hydroxylamine hydrochloride / 2-ethoxy-ethanol / 0.5 h / Microwave irradiation

3: pyridine / 1 h / 20 °C

With pyridine; hydroxylamine hydrochloride; potassium carbonate; In 2-ethoxy-ethanol;
DOI:10.1016/j.bmc.2012.05.035

Reference yield:

: 1135132-09-0
6-(4-acetylphenylamino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one

: 1390649-38-3
(E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride / 2-ethoxy-ethanol / 0.5 h / Microwave irradiation

2: pyridine / 1 h / 20 °C

With pyridine; hydroxylamine hydrochloride; In 2-ethoxy-ethanol;
DOI:10.1016/j.bmc.2012.05.035