(E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime

Base Information

• Chemical Name: (E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime
• CAS No.: 1390649-36-1
• Molecular Formula: C₂₅H₂₀N₄O₃
• Molecular Weight: 424.459

Synonyms:(E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime

Chemical Property of (E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime

Chemical Property:

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Technology Process of (E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime

There total 2 articles about (E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-aminobenzophenone (99-92-3) → (E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime (1390649-36-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / 2-ethoxy-ethanol / 1 h / Microwave irradiation

2: hydroxylamine hydrochloride / 2-ethoxy-ethanol / 0.5 h / Microwave irradiation

With hydroxylamine hydrochloride; potassium carbonate; In 2-ethoxy-ethanol;

DOI:10.1016/j.bmc.2012.05.035

Reference yield:

6-chloro-9-methoxy-11H-indeno[1,2-c]quinolin-11-one (191801-89-5) → (E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime (1390649-36-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / 2-ethoxy-ethanol / 1 h / Microwave irradiation

2: hydroxylamine hydrochloride / 2-ethoxy-ethanol / 0.5 h / Microwave irradiation

With hydroxylamine hydrochloride; potassium carbonate; In 2-ethoxy-ethanol;

DOI:10.1016/j.bmc.2012.05.035

Reference yield: 82.0%

(E)-6-((4-[(E)-1-(hydroximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one oxime (1390649-36-1) + acetic anhydride (108-24-7) → (E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime (1390649-38-3)

Guidance literature:

With pyridine; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2012.05.035

upstream raw materials:

6-chloro-9-methoxy-11H-indeno[1,2-c]quinolin-11-one

p-aminobenzophenone

Downstream raw materials:

(E)-6-((4-[(E)-1-(acetoximino)ethyl]phenyl)amino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one O-acetyloxime

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