2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

Base Information

Chemical Name:2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril
CAS No.:75410-50-3
Molecular Formula:C₂₁H₂₃NO₁₀
Molecular Weight:449.414
Hs Code.:

Synonyms:2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

Suppliers and Price of 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

There total 10 articles about 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 75410-49-0
2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid

: 75410-50-3
2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

Guidance literature:: With pyridine; trifluoroacetic anhydride; for 2h; Ambient temperature;

Reference yield: 21.0%

: 72692-06-9,73464-50-3,3082-95-9
methyl 2,3,4-tri-O-acetyl-D-glucopyranuronate

: 532-28-5,613-88-7
(RS)-mandelonitrile

: 75410-50-3
2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 4 ℃; for 72h;
DOI:10.1021/jo00199a046

Reference yield:

: 4410-31-5,24008-62-6,24008-63-7,4358-86-5
(RS)-mandelamide

: 75410-50-3,83462-71-9,83462-73-1,100836-93-9
D-2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

Guidance literature:: Multi-step reaction with 2 steps

1: HgBr₂/Hg(CN)2 / 1,2-dichloro-ethane / 84 °C

2: pyridine, (CF₃CO)2O / 2 h / Ambient temperature

With pyridine; mercury(II) cyanide; trifluoroacetic anhydride; mercury dibromide; In 1,2-dichloro-ethane;