2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid

Base Information

• Chemical Name: 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid
• CAS No.: 75410-49-0
• Molecular Formula: C₂₁H₂₅NO₁₁
• Molecular Weight: 467.43

Synonyms:2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid

Chemical Property of 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid

Chemical Property:

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Technology Process of 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid

There total 3 articles about 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

(RS)-mandelamide (4410-31-5,24008-62-6,24008-63-7,4358-86-5) + 1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester (21085-72-3) → 2-(Methyl-di-O-acetyl-α-D-glucopyranuronosyl-1,2-acetylidenoxy)-2-phenylacetamid (83441-69-4) + 2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid (75410-49-0)

Guidance literature:

With mercury(II) cyanide; mercury dibromide; In 1,2-dichloro-ethane; at 84 ℃;

Reference yield: 5.8%

(RS)-mandelamide (4410-31-5,24008-62-6,24008-63-7,4358-86-5) + 1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester (21085-72-3) → 2-(Methyl-di-O-acetyl-α-D-glucopyranuronosyl-1,2-acetylidenoxy)-2-phenylacetamid (83441-69-4) + D-2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid (75410-49-0,83462-70-8,83462-72-0) + L-2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid (75410-49-0,83462-70-8,83462-72-0)

Guidance literature:

With mercury(II) cyanide; mercury dibromide; In 1,2-dichloro-ethane; at 84 ℃;

Reference yield: 5.8%

(RS)-mandelamide (4410-31-5,24008-62-6,24008-63-7,4358-86-5) + 1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester (21085-72-3) → 2-(Methyl-di-O-acetyl-α-D-glucopyranuronosyl-1,2-acetylidenoxy)-2-phenylacetamid (83441-69-4) + D-2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid (75410-49-0,83462-70-8,83462-72-0) + L-2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetamid (75410-49-0,83462-70-8,83462-72-0)

Guidance literature:

With mercury(II) cyanide; mercury dibromide; In 1,2-dichloro-ethane; at 84 ℃;

upstream raw materials:

(RS)-mandelamide

1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

Downstream raw materials:

Mandelnitril-β-D-glucuronid

2-(Methyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

2-(2,3,4-Tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

L-2-(Methyl-2,3,4-tri-O-acetyl-β-D-glucopyranuronosyloxy)-2-phenylacetonitril

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