2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine

Base Information

Chemical Name:2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine
CAS No.:101527-64-4
Molecular Formula:C₂₉H₂₉ClN₂O₇S
Molecular Weight:585.077
Hs Code.:

Synonyms:2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine

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Chemical Property of 2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine

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Technology Process of 2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine

There total 3 articles about 2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.6%

: 101552-16-3
2',3'-di-O-mesyl-5'-O-trityl-2',3'-seco-uridine

: 101527-64-4
2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine

Guidance literature:: With hydrogenchloride; In N,N-dimethyl-formamide; for 5h; Ambient temperature;
DOI:10.1002/hlca.19920750209

Reference yield: 76.0%

: O²,2'-anhydro-3'-O-mesyl-5'-O-trityl-2',3'-secouridine

: 101527-64-4
2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine

Guidance literature:: With hydrogenchloride; In N,N-dimethyl-formamide; for 5h; Ambient temperature;

Reference yield:

: 101527-47-3
1-(2-hydroxy-1-{[1-hydroxy-3-(triphenylmethoxy)propan-2-yl]oxy}ethyl)pyrimidine-2,4(1H,3H)-dione

: 101527-64-4
2'-chloro-2'-deoxy-3'-O-(methylsulfonyl)-5'-O-(triphenylmethyl)-2',3'-secouridine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / 18 h / 4 °C

2: 88.6 percent / 2 N aq. HCl / dimethylformamide / 5 h / Ambient temperature

With pyridine; hydrogenchloride; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19920750209