N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride

Base Information

Chemical Name:N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride
CAS No.:1307309-93-8
Molecular Formula:C₂₂H₄₁N₃O₂*ClH
Molecular Weight:416.047
Hs Code.:

Synonyms:N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride

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Chemical Property of N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride

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Technology Process of N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride

There total 3 articles about N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1307309-92-7
N-(1-cyanocyclopropyl)-11-(cyclohexylmethoxy)undecanamide

: 1307309-93-8
N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride

Guidance literature:: N-(1-cyanocyclopropyl)-11-(cyclohexylmethoxy)undecanamide; With sodium methylate; In methanol; at 20 - 50 ℃; for 24h; Inert atmosphere;

With ammonium chloride; In methanol; at 50 ℃; Inert atmosphere;
DOI:10.1021/jm2001053

Reference yield:

: 1307309-91-6
11-(cyclohexylmethoxy)undecanoic acid

: 1307309-93-8
N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere

2.1: sodium methylate / methanol / 24 h / 20 - 50 °C / Inert atmosphere

2.2: 50 °C / Inert atmosphere

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium methylate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/jm2001053

Reference yield:

: 100-49-2
cyclohexylmethyl alcohol

: 1307309-93-8
N-(1-carbamimidoylcyclopropyl)-11-(cyclohexylmethoxy)undecanamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 - 20 °C / Inert atmosphere

1.2: 12 h / Inert atmosphere

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere

3.1: sodium methylate / methanol / 24 h / 20 - 50 °C / Inert atmosphere

3.2: 50 °C / Inert atmosphere

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium methylate; sodium hydride; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil; 1.1: Williamson synthesis / 1.2: Williamson synthesis;
DOI:10.1021/jm2001053