bis[((2,3,4,5,6-pentafluorobenzyl)dimethylsilyl)cyclopentadienyl]zirconium dichloride

Base Information

Chemical Name:bis[((2,3,4,5,6-pentafluorobenzyl)dimethylsilyl)cyclopentadienyl]zirconium dichloride
CAS No.:850146-27-9
Molecular Formula:C₂₈H₂₄Cl₂F₁₀Si₂Zr
Molecular Weight:768.784
Hs Code.:

Synonyms:bis[((2,3,4,5,6-pentafluorobenzyl)dimethylsilyl)cyclopentadienyl]zirconium dichloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[((2,3,4,5,6-pentafluorobenzyl)dimethylsilyl)cyclopentadienyl]zirconium dichloride

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Technology Process of bis[((2,3,4,5,6-pentafluorobenzyl)dimethylsilyl)cyclopentadienyl]zirconium dichloride

There total 1 articles about bis[((2,3,4,5,6-pentafluorobenzyl)dimethylsilyl)cyclopentadienyl]zirconium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 850146-33-7
[(2,3,4,5,6-pentafluorobenzyl)dimethylsilyl]cyclopentadiene

: 10026-11-6
zirconium(IV) chloride

: 850146-27-9
bis[((2,3,4,5,6-pentafluorobenzyl)dimethylsilyl)cyclopentadienyl]zirconium dichloride

Guidance literature:: With n-BuLi; In diethyl ether; hexane; (N2); Schlenk technique; BuLi/C6H14 added to Si compd./C6H14 at 0°C; left (0°C, 30 min); warmed to ambient temp.; left for 2 h; filtered; rinsed (C5H12); dried (vac.); dissolved in Et2O; solid ZrCl4 added; left at ambient temp. overnight; filtered; solvent removed (vac.); elem. anal.;
DOI:10.1021/om049507z