(1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide

Base Information

Chemical Name:(1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide
CAS No.:152534-40-2
Molecular Formula:C₂₀H₂₅N₃O₃
Molecular Weight:355.437
Hs Code.:

Synonyms:(1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide

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Technology Process of (1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide

There total 4 articles about (1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 90175-94-3
N-1-(2,3-dihydro-3-oxopyridazin-6-yl)ethylamine hydrochloride

: 7-benzoylheptanoyl chloride

: 152534-40-2
(1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/jm00076a005

Reference yield:

: 68219-65-8
5-Benzamido-4-oxohexansaeureethylester

: 152534-40-2
(1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide

Guidance literature:: Multi-step reaction with 4 steps

1: N₂H₄*H₂O / ethanol / Heating

2: Br₂, AcOH / 40 °C

3: 82 percent / 6M aq. HCl / 18 h / Heating

4: 61 percent / Et₃N / dimethylformamide / 24 h / 20 °C

With hydrogenchloride; bromine; hydrazine hydrate; acetic acid; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00076a005

Reference yield:

: 68219-76-1
6-(1-benzoylamino-ethyl)-2H-pyridazin-3-one

: 152534-40-2
(1'RS)-N-<1-(1,6-dihydro-6-oxo-3-pyridazinyl)ethyl>-8-oxo-8-phenyloctanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 6M aq. HCl / 18 h / Heating

2: 61 percent / Et₃N / dimethylformamide / 24 h / 20 °C

With hydrogenchloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00076a005