Technology Process of 6-<4-(2-bromoethyl)benzenesulfonamido>saccharin
There total 5 articles about 6-<4-(2-bromoethyl)benzenesulfonamido>saccharin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; hydroquinone;
In
water; acetonitrile;
for 12h;
Ambient temperature;
DOI:10.1246/bcsj.55.3824
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ClSO3H / 24 h / 60 - 70 °C
2: conc. aq. NH3 / diethyl ether / 2 h / Heating
3: 56 percent / CrO3, conc. H2SO4 / H2O / 24 h / Ambient temperature
4: 63 percent / cyclohexene / 5percent Pd/C / ethanol / 2 h / Heating
5: 27 percent / NaOH, hydroquinone / H2O; acetonitrile / 12 h / Ambient temperature
With
chromium(VI) oxide; chlorosulfonic acid; ammonium hydroxide; sodium hydroxide; sulfuric acid; hydroquinone; cyclohexene;
palladium on activated charcoal;
In
diethyl ether; ethanol; water; acetonitrile;
DOI:10.1246/bcsj.55.3824
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 56 percent / CrO3, conc. H2SO4 / H2O / 24 h / Ambient temperature
2: 63 percent / cyclohexene / 5percent Pd/C / ethanol / 2 h / Heating
3: 27 percent / NaOH, hydroquinone / H2O; acetonitrile / 12 h / Ambient temperature
With
chromium(VI) oxide; sodium hydroxide; sulfuric acid; hydroquinone; cyclohexene;
palladium on activated charcoal;
In
ethanol; water; acetonitrile;
DOI:10.1246/bcsj.55.3824
