2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

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Chemical Name:2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole
CAS No.:314286-45-8
Molecular Formula:C₅₅H₅₉NO₄S₇
Molecular Weight:1022.54
Hs Code.:

2-{4-[2-(2-{4-[bis-(4-<i>tert</i>-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5<i>H</i>-[1,3]dithiolo[4,5-<i>c</i>]pyrrole

Synonyms:2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

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Chemical Property of 2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

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Technology Process of 2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

There total 12 articles about 2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 177609-52-8
2-(2-{4-[bis(4-tert-butylphenyl)-(4-ethylphenyl)methyl]phenoxy}ethoxy)ethanol

: 314286-45-8
2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

2: 99 percent / NaI / acetone / 14 h / Heating

3: 1.32 g / tetrahydrofuran; methanol / 20 h / 20 °C

With sodium hydroxide; sodium iodide; In tetrahydrofuran; methanol; water; acetone;
DOI:10.1021/ja0114456

Reference yield:

: 177609-49-3
bis(4-tert-butylphenyl)(4-ethylphenyl)(4-hydroxyphenyl)methane

: 314286-45-8
2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: Multi-step reaction with 5 steps

1: KOH; LiBr / butan-1-ol / 60 h / Heating

2: 9.90 g / aq. HCl / methanol; CH₂Cl₂ / 2.5 h / 20 °C

3: 53 percent / NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

4: 99 percent / NaI / acetone / 14 h / Heating

5: 1.32 g / tetrahydrofuran; methanol / 20 h / 20 °C

With hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium iodide; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; butan-1-ol;
DOI:10.1021/ja0114456

Reference yield:

: 2-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

: 314286-45-8
2-{4-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethylsulfanyl]-5-methylsulfanyl-[1,3]dithiol-2-ylidene}-5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: 9.90 g / aq. HCl / methanol; CH₂Cl₂ / 2.5 h / 20 °C

2: 53 percent / NaOH / tetrahydrofuran; H₂O / 4 h / 0 °C

3: 99 percent / NaI / acetone / 14 h / Heating

4: 1.32 g / tetrahydrofuran; methanol / 20 h / 20 °C

With hydrogenchloride; sodium hydroxide; sodium iodide; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1021/ja0114456