n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside
CAS No.:872594-11-1
Molecular Formula:C₂₃H₂₈O₇S₂
Molecular Weight:480.603
Hs Code.:

Synonyms:n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

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Technology Process of n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

There total 5 articles about n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872594-07-5
n-propyl 4,6-O-benzylidene-1-thiol-β-D-glucopyranoside

: 98-59-9
p-toluenesulfonyl chloride

: 872594-11-1
n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1021/ol052128x

Reference yield:

: 872594-07-5
n-propyl 4,6-O-benzylidene-1-thiol-β-D-glucopyranoside

: 98-59-9
p-toluenesulfonyl chloride

: 872594-11-1
n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

: n-propyl 4,6-O-benzylidene-2-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

Guidance literature:: With potassium iodide; silver(l) oxide; In dichloromethane; at 20 ℃; for 2h; Title compound not separated from byproducts;
DOI:10.1021/ol052128x

Reference yield:

: (2R,3S,4S,5R)-2-Hydroxymethyl-6-propylsulfanyl-tetrahydro-pyran-3,4,5-triol

: 872594-11-1
n-propyl 4,6-O-benzylidene-3-O-p-toluenesulfonyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: CSA / acetonitrile

2: pyridine / CH₂Cl₂ / 20 °C

With pyridine; camphor-10-sulfonic acid; In dichloromethane; acetonitrile;
DOI:10.1021/ol052128x