metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato

Base Information

• Chemical Name: metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato
• CAS No.: 93371-95-0
• Molecular Formula: C₁₇H₁₅NO₃S
• Molecular Weight: 313.377
• Mol file: 93371-95-0.mol

Synonyms:metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato

Chemical Property of metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato

There total 3 articles about metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methyl 2-(4-aminophenyl)propanoate (39718-97-3) + 2-chlorosulfenylbenzoyl chloride (3950-02-5) → metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato (93371-95-0)

Guidance literature:

In pyridine; at 50 ℃; for 0.333333h;

Reference yield:

2,2'-dithiobenzoic acid (119-80-2) → metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato (93371-95-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) SOCl₂; 2.) Cl₂ / 1.) reflux; 2.) CCl₄

2: 80 percent / pyridine / 0.33 h / 50 °C

With pyridine; thionyl chloride; chlorine;

Reference yield:

2,2'-dithiodibenzoic acid dichloride (19602-82-5) → metile 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionato (93371-95-0)

Guidance literature:

Multi-step reaction with 2 steps

1: Cl₂ / CCl₄ / Ambient temperature

2: 85 percent / pyridine / 0.33 h / 50 °C

With chlorine; In pyridine; tetrachloromethane;

upstream raw materials:

methyl 2-(4-aminophenyl)propanoate

2-chlorosulfenylbenzoyl chloride

2,2'-dithiodibenzoic acid dichloride

2,2'-dithiobenzoic acid

Downstream raw materials:

2-<4-(1-carbossietil)fenil>-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

2-<4-(1-metossicarboniletil)fenil>-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

acido 2-<4-(3-oxo-1,2-benzisotiazolin-2-il)fenil>propionico