6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate

Base Information

Chemical Name:6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate
CAS No.:170512-22-8
Molecular Formula:C₄₁H₄₈O₇S
Molecular Weight:684.894
Hs Code.:

Synonyms:6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate

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Technology Process of 6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate

There total 6 articles about 6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 124-63-0
methanesulfonyl chloride

: 170512-20-6
6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexan-1-ol

: 170512-22-8
6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1248/cpb.43.1407

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 170512-22-8
6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / p-TsOH*H₂O / benzene / 3 h / Heating

2: 82 percent / NaH, 1,3-dimethyl-2-imidazolidinone / tetrahydrofuran / 12 h / Ambient temperature

3: 95 percent / LiAlH₄ / diethyl ether / 0.25 h / Ambient temperature

4: 99 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With 1,3-dimethyl-2-imidazolidinone; lithium aluminium tetrahydride; sodium hydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.43.1407

Reference yield:

: 159454-99-6
ethyl 4,4-dimethoxycyclohexylideneacetate

: 170512-22-8
6,6-dibenzyloxy-2-(4,4-dibenzyloxy-1-cyclohexenyl)hexyl methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / p-TsOH*H₂O, MS 3A / hexane / 22 h / Ambient temperature

2: 82 percent / NaH, 1,3-dimethyl-2-imidazolidinone / tetrahydrofuran / 12 h / Ambient temperature

3: 95 percent / LiAlH₄ / diethyl ether / 0.25 h / Ambient temperature

4: 99 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With 1,3-dimethyl-2-imidazolidinone; lithium aluminium tetrahydride; sodium hydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1248/cpb.43.1407