diethyl α-truxillate

Base Information

Chemical Name:diethyl α-truxillate
CAS No.:55631-79-3
Molecular Formula:C₂₂H₂₄O₄
Molecular Weight:352.43
Hs Code.:

Synonyms:diethyl α-truxillate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl α-truxillate

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Technology Process of diethyl α-truxillate

There total 10 articles about diethyl α-truxillate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: tin tetrachloride-bis{(E)-ethyl cinnamate}

: 55631-79-3
diethyl α-truxillate

Guidance literature:: In solid; byproducts: (Z)-ethyl cinnamate, (E)-ethyl cinnamate; Irradiation (UV/VIS); irradiated (313 nm) for 12 h at 0°C; N2 atm.; topochemical reaction control; <1% Z-ethyl cinnamate, 14% E-ethyl cinnamate; 34% conversion to α-truxillate after 5 h irradiation; reaction product quenched with water, org. materials extracted with CH2Cl2, dried over MgSO4, soln. concd.; product anal. by GC/MS and (1)H-NMR;
DOI:10.1021/ja00212a039

Reference yield: 14.0%

: 55631-79-3
diethyl α-truxillate

: 4192-77-2
ethyl cinnamate

Guidance literature:: at 0 ℃; for 12h; Irradiation;
DOI:10.1021/ja00212a039

Reference yield: 3.0%

: 4192-77-2
ethyl cinnamate

: 55631-79-3
diethyl α-truxillate

Guidance literature:: at 0 ℃; for 5h; Product distribution; Irradiation; solid-state photodimerization; other cinnamic esters; reaction of complexes with different Lewis acids;
DOI:10.1021/ja00212a039