methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate

Base Information

Chemical Name:methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate
CAS No.:1072937-66-6
Molecular Formula:C₂₁H₁₉BrO₇
Molecular Weight:463.282
Hs Code.:

Synonyms:methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate

Suppliers and Price of methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate

There total 1 articles about methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1072937-60-0
3-bromo-5-formyl-2-methoxybenzoic acid methyl ester

: 83908-12-7
(3-acetoxy-4-methoxycarbonylbenzyl)triphenylphosphonium bromide

: 1072937-67-7
methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-hydroxybenzoate

: 1072937-66-6
methyl 4-[(E)-2-(5-bromo-3-methoxycarbonyl-4-methoxyphenyl)vinyl]-2-acetoxybenzoate

Guidance literature:: (3-acetoxy-4-methoxycarbonylbenzyl)triphenylphosphonium bromide; With lithium diisopropyl amide; In tetrahydrofuran; cyclohexane; at -75 - 0 ℃;

3-bromo-5-formyl-2-methoxybenzoic acid methyl ester; In tetrahydrofuran; cyclohexane; at -75 - 20 ℃;

With iodine; In n-heptane; Further stages.; Heating;
DOI:10.1016/j.bmc.2008.07.090