4-hexadecyl-1-trimethylsilylethynylbenzene

Base Information

Chemical Name:4-hexadecyl-1-trimethylsilylethynylbenzene
CAS No.:181523-33-1
Molecular Formula:C₂₇H₄₆Si
Molecular Weight:398.748
Hs Code.:

Synonyms:4-hexadecyl-1-trimethylsilylethynylbenzene

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Chemical Property of 4-hexadecyl-1-trimethylsilylethynylbenzene

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Technology Process of 4-hexadecyl-1-trimethylsilylethynylbenzene

There total 4 articles about 4-hexadecyl-1-trimethylsilylethynylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116526-71-7
1-(4-bromophenyl)hexadecan-1-one

: 181523-33-1
4-hexadecyl-1-trimethylsilylethynylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate; potassium hydroxide / octanol / 3 h / Reflux; Inert atmosphere

2: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / 50 - 80 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; hydrazine hydrate; triethylamine; potassium hydroxide; In octanol; 1: Wolf-Kishner reaction / 2: Sonogashira coupling;
DOI:10.1021/ma101709h

Reference yield:

: 112-67-4
n-hexadecanoyl chloride

: 181523-33-1
4-hexadecyl-1-trimethylsilylethynylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 1 h / 60 °C / Inert atmosphere

2: hydrazine hydrate; potassium hydroxide / octanol / 3 h / Reflux; Inert atmosphere

3: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / 50 - 80 °C / Inert atmosphere

With aluminum (III) chloride; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; hydrazine hydrate; triethylamine; potassium hydroxide; In octanol; 1: Friedel Crafts acylation / 2: Wolf-Kishner reaction / 3: Sonogashira coupling;
DOI:10.1021/ma101709h

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 181523-33-1
4-hexadecyl-1-trimethylsilylethynylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 1 h / 60 °C / Inert atmosphere

2: hydrazine hydrate; potassium hydroxide / octanol / 3 h / Reflux; Inert atmosphere

3: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / 50 - 80 °C / Inert atmosphere

With aluminum (III) chloride; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; hydrazine hydrate; triethylamine; potassium hydroxide; In octanol; 1: Friedel Crafts acylation / 2: Wolf-Kishner reaction / 3: Sonogashira coupling;
DOI:10.1021/ma101709h