2-Cyano-4,4,4-trifluoro-3--2-butenonitrile

Base Information

Chemical Name:2-Cyano-4,4,4-trifluoro-3--2-butenonitrile
CAS No.:339348-85-5
Molecular Formula:C₁₂H₈F₃N₃O
Molecular Weight:267.21
Hs Code.:

2-Cyano-4,4,4-trifluoro-3-<N-(4-methoxyphenyl)amino>-2-butenonitrile

Synonyms:2-Cyano-4,4,4-trifluoro-3--2-butenonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyano-4,4,4-trifluoro-3--2-butenonitrile

Chemical Property:

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Technology Process of 2-Cyano-4,4,4-trifluoro-3--2-butenonitrile

There total 3 articles about 2-Cyano-4,4,4-trifluoro-3--2-butenonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75999-66-5
N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

: 109-77-3
malononitrile

: 339348-85-5
2-Cyano-4,4,4-trifluoro-3--2-butenonitrile

Guidance literature:: With sodium hydride; In acetonitrile; for 0.5h; Microwave irradiation;
DOI:10.1055/s-0037-1609433

Reference yield: 94.0%

: 75999-66-5
(Z)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidoyl chloride

: 109-77-3
malononitrile

: 339348-85-5
2-Cyano-4,4,4-trifluoro-3--2-butenonitrile

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1021/jo00086a053

Reference yield:

: 104-94-9
4-methoxy-aniline

: 339348-85-5
2-Cyano-4,4,4-trifluoro-3--2-butenonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; triphenylphosphine; tetrachloromethane / Reflux

2: sodium hydride / acetonitrile / 0.5 h / Microwave irradiation

With tetrachloromethane; sodium hydride; triethylamine; triphenylphosphine; In acetonitrile;
DOI:10.1055/s-0037-1609433