methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

Base Information

Chemical Name:methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester
CAS No.:933442-95-6
Molecular Formula:C₃₈H₄₉N₃O₉S₃
Molecular Weight:788.02
Hs Code.:

methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

Synonyms:methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

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Chemical Property of methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

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Technology Process of methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

There total 4 articles about methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 933442-94-5
C₃₇H₄₇N₃O₇S₂

: 124-63-0
methanesulfonyl chloride

: 933442-95-6
methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo0619837

Reference yield:

: 933442-93-4
C₅₆H₆₁N₃O₇S₂

: 933442-95-6
methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / trifluoroacetic acid / methanol; CH₂Cl₂ / 12 h / 20 °C

2: 100 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With triethylamine; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/jo0619837

Reference yield:

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 933442-95-6
methanesulfonic acid 6-[{2-[[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / cesium carbonate; tetrabutylammonium bromide / toluene / Heating

2: 90 percent / trifluoroacetic acid / methanol; CH₂Cl₂ / 12 h / 20 °C

3: 100 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With tetrabutylammomium bromide; caesium carbonate; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; toluene;
DOI:10.1021/jo0619837