3--(E)-2-propen-1-ol

Base Information

Chemical Name:3--(E)-2-propen-1-ol
CAS No.:137571-44-9
Molecular Formula:C₁₅H₂₂O₂
Molecular Weight:234.338
Hs Code.:

3-<m-(3-Methyl-4-hydroxypentyl)phenyl>-(E)-2-propen-1-ol

Synonyms:3--(E)-2-propen-1-ol

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Chemical Property of 3--(E)-2-propen-1-ol

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Technology Process of 3--(E)-2-propen-1-ol

There total 8 articles about 3--(E)-2-propen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-36-5
1-methoxycarbonyl-3-methylbenzene

: 137571-44-9
3--(E)-2-propen-1-ol

Guidance literature:: Multi-step reaction with 8 steps

1: N-bromosuccinimide, benzoyl peroxide / CCl₄ / 3 h / Heating

2: NEt₃ / tetrahydrofuran / 1.5 h / 0 °C

3: 82 percent / LiAlH₄ / diethyl ether / 2 h / 0 °C

4: 1) n-BuLi / 1) THF, hexane, -78 deg C, 15 min, 2a) -78 deg C, 5 min, b) to r.t.

5: 89 percent / n-Bu₃SnH, AIBN / benzene / 2.5 h / Heating

6: 1) Me₂S*BH₃, 2) 3 N NaOH, H₂O₂ / 1) THF, Et₂O, -20 deg C, 2) MeOH

7: activated MnO₂ / CHCl₃

8: tetrahydrofuran / Ambient temperature

With manganese(IV) oxide; sodium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; Perbenzoic acid; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; dihydrogen peroxide; tri-n-butyl-tin hydride; triethylamine; In tetrahydrofuran; tetrachloromethane; diethyl ether; chloroform; benzene;
DOI:10.1021/jo00029a033

Reference yield:

: 137624-78-3
m-(4-Hydroxy-3-methylpentyl)benzyl alcohol

: 137571-44-9
3--(E)-2-propen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: activated MnO₂ / CHCl₃

2: tetrahydrofuran / Ambient temperature

With manganese(IV) oxide; In tetrahydrofuran; chloroform;
DOI:10.1021/jo00029a033

Reference yield:

: 137571-41-6
m-<(E)-3-Methyl-3-pentenyl>benzyl alcohol

: 137571-44-9
3--(E)-2-propen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Me₂S*BH₃, 2) 3 N NaOH, H₂O₂ / 1) THF, Et₂O, -20 deg C, 2) MeOH

2: activated MnO₂ / CHCl₃

3: tetrahydrofuran / Ambient temperature

With manganese(IV) oxide; sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide; In tetrahydrofuran; chloroform;
DOI:10.1021/jo00029a033