di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate

Base Information

Chemical Name:di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate
CAS No.:100839-22-3
Molecular Formula:C₂₄H₃₉NO₅
Molecular Weight:421.577
Hs Code.:

Synonyms:di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate

Suppliers and Price of di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate

There total 2 articles about di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 100839-16-5
di-tert-butyl-2-(4-methoxyphenyl)-1,1-cyclopropanedicarboxylate

: 109-89-7
diethylamine

: 100839-22-3
di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate

Guidance literature:: With diethylaluminium chloride; In toluene; at 110 ℃; for 2h;
DOI:10.1021/jo00358a045

Reference yield:

: 35207-75-1
di-tert-butyl diazomalonate

: 100839-22-3
di-tert-butyl 2-<2-(diethylamino)-2-(4-methoxyphenyl)ethyl>propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CuI*P(OMe)3 / 1.) 100 deg C, 2.) toluene, reflux, 45 min

2: 89 percent / Et₂AlCl / toluene / 2 h / 110 °C

With CuI*P(OMe)₃; diethylaluminium chloride; In toluene;
DOI:10.1021/jo00358a045