2-benzoyloxy-4,5-dimethylnitrobenzene

Base Information

• Chemical Name: 2-benzoyloxy-4,5-dimethylnitrobenzene
• CAS No.: 196494-43-6
• Molecular Formula: C₁₅H₁₃NO₄
• Molecular Weight: 271.273
• Mol file: 196494-43-6.mol

Synonyms:2-benzoyloxy-4,5-dimethylnitrobenzene

Chemical Property of 2-benzoyloxy-4,5-dimethylnitrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-benzoyloxy-4,5-dimethylnitrobenzene

There total 3 articles about 2-benzoyloxy-4,5-dimethylnitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dimethylphenyl benzoate (3845-63-4) → 2-benzoyloxy-4,5-dimethylnitrobenzene (196494-43-6)

Guidance literature:

With sulfuric acid; nitric acid; a) from 0 deg C to RT, 1 h, b) 50 deg C, 20 min;

DOI:10.1055/s-1997-1290

Reference yield:

3,4-Dimethylphenol (95-65-8) → 2-benzoyloxy-4,5-dimethylnitrobenzene (196494-43-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 1 h

2: conc. HNO₃, conc. H₂SO₄ / a) from 0 deg C to RT, 1 h, b) 50 deg C, 20 min

With pyridine; sulfuric acid; nitric acid;

DOI:10.1055/s-1997-1290

Reference yield:

benzoyl chloride (98-88-4) → 2-benzoyloxy-4,5-dimethylnitrobenzene (196494-43-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 1 h

2: conc. HNO₃, conc. H₂SO₄ / a) from 0 deg C to RT, 1 h, b) 50 deg C, 20 min

With pyridine; sulfuric acid; nitric acid;

DOI:10.1055/s-1997-1290

upstream raw materials:

3,4-dimethylphenyl benzoate

3,4-Dimethylphenol

benzoyl chloride

Downstream raw materials:

3-(2-hydroxy-4,5-dimethylphenylamino)-1,1,4,4-tetramethyltetralin-2-one

2-amino-4,5-dimethylphenol

4,5-dimethyl-2-nitrophenol