Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester

Base Information

Chemical Name:Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester
CAS No.:905268-95-3
Molecular Formula:C₂₉H₃₉NO₅Si
Molecular Weight:509.718
Hs Code.:

Synonyms:Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester

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Chemical Property of Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester

Chemical Property:

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Technology Process of Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester

There total 5 articles about Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 905268-94-2
Acetic acid (1R,4S)-4-[3-(tert-butyl-diphenyl-silanyloxy)-propylamino]-cyclopent-2-enyl ester

: 541-41-3
chloroformic acid ethyl ester

: 905268-95-3
Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1021/jo060555y

Reference yield:

: Acetic acid (1R,4S)-4-[3-(tert-butyl-diphenyl-silanyloxy)-prop-(E)-ylideneamino]-cyclopent-2-enyl ester

: 905268-95-3
Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 6.90 g / NaBH₄ / CH₂Cl₂; methanol / 0.33 h / 20 °C

2: 90 percent / pyridine / CH₂Cl₂

With pyridine; sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1021/jo060555y

Reference yield:

: 201054-55-9,154802-92-3,178152-48-2
(+)-(1R,4S)-1-hydroxy-4-[(tert-butoxycarbonyl)amino]-2-cyclopentene

: 905268-95-3
Acetic acid (1R,4S)-4-{[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-ethoxycarbonyl-amino}-cyclopent-2-enyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / imidazole / CH₂Cl₂

2: trifluoroacetic acid / CH₂Cl₂ / 2 h / 20 °C

3: Na₂SO₄ / CH₂Cl₂ / 12.5 h / -20 - 20 °C

4: 6.90 g / NaBH₄ / CH₂Cl₂; methanol / 0.33 h / 20 °C

5: 90 percent / pyridine / CH₂Cl₂

With pyridine; 1H-imidazole; sodium tetrahydroborate; sodium sulfate; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/jo060555y